INSTRUMENTAL ANALYSIS AND CHEMICAL FOOD ANALYSIS
 
Taught in 3rd year Bachelor in Biosciences Food Industry
Linking course : Master in Biosciences,Agricultural science - Food Industry for Prof.Bach. in agro- en biotechnologie (alle afst.)
Linking course : Master in Biosciences,Agricultural science - Food Industry for Prof.Bach. in biomed. Labtechnologie
Linking course : Master in Biosciences,Agricultural science - Food Industry for Prof.Bach. in chemistry
Linking course : Master in Biosciences,Agricultural science - Food Industry for Prof.Bach. in voeding- en dieetkunde
Theory [A] 24.0
Exercises [B] 24.0
Training and projects [C] 12.0
Studytime [D] 150.0
Studypoints [E] 5
Level specialized
Credit contract? Unrestricted access
Examination contract?
Language of instruction Dutch
Lecturer Joseph SCHAUBROECK
Reference BBBIOW03A00017
 
Key words
Instrumental techniques - food analysis

Objectives
The main objective is to provide a more solid and profound scientifically basis (fysico-chemical) which in practice gives access to the application of a great variety of qualitative and quantitative applied analytical methods usefull in food analysis.

Topics
Theory:
  • Instrumental characteristics
  • Electrochemical methods: conductometry, potentiometry, electrolysis, voltammetry, amperometry, coulometry
  • Optical methods: interaction electromagnetic radiation (matter,molecular and atomic absorption/emission (UV - VIS, IR, FT-IR, NIRA, RAMAN, turbidimetry, nefelometry, refractometry, polarometry, flame photometry, ICP, AES, AAS, XRF, chemiluminescence,... (depending on timeschedule)
  • NMR and MS
The analytical methods are illustrated with applications in food analysis.

Exercises
  • GC: determination of fats
  • HPLC:determination of vit C ( extern en intern standardisation )
  • Spectroscopy: fluorimetric determination quinine in tonic
  • TLC: determination of biphenyl en ortho phenyl phenol in citrusfruits
  • ISE: use of ion selective electrode (determination nitrate in vegetables)
  • extern standard en multiple standardaddition
  • Demonstrations: GCMS , SPE en SPME
C-hours : productquality, quality-assurance and legislation

Prerequisites
Basic knowledge of inorganic - organic chemistry (candidatures) and analytical chemistry (chemical analysis)

Final Objectives
  • The student has to think and argue in a logical, critical and scientific manner and to implement scientific insights on related problems. At the same time he must be able to communicate verbal and/or written in an efficient manner;
  • The student must have insight to the different scientific/technical disciplines;
  • The students have to perform quality minded and has to take care of the environmental - , safety- and health aspects;
  • The students must obtain a clear insight into chemical general knowledge and basic skills and must be able to link the different aspects and apply them in process- and productcontrol;
  • Via the practical exercises, the mentioned objectives are persuited and other qualifications as team spirit are also emphasized.


Materials used
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teacher's courses - background information
scientific & technical literature - school library materials...

Study costs
Cost: 70.0 EUR
Theory syllabus: about € 15
Exercises: syllabus, laboratory-coat, safety glasses, pippetor,…: about € 50
Exercises: syllabus only: about € 5

Study guidance
Supplementary support and explanation is provided by appointment

Teaching Methods
Lectures - demonstrations - exercises - individual reports - discussion exercises - home study - training period

Assessment
Theory: Combination of written and oral examination
Exercises: permanent evaluation, tasks
C- hours: permanent evaluation, tasks

Coefficient:
Theory: ± 57 %
Exercises: ± 29 %
C-hours: ± 14 %


Lecturer(s)
Theory: Dr.J. Schaubroeck
Exercises: Ing. P. Maene